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All Journal Indonesia Chimica Acta Chemistry Indonesian Journal of Chemical Research
Serly Jolanda Sekewael
Chemistry Department, Faculty Of Mathematics And Natural Sciences Pattimura University, Kampus Poka, Jl. Ir. M. Putuhena, Ambon 97134, Indonesia
Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Engineering Environmental Science

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Journal : Indonesia Chimica Acta

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Karakterisasi Sifat Fisikokimia Komposit Besi Oksida-Montmorilonit Hasil Interkalasi Silikat Lempung Montmorilonit Serly Jolanda Sekewael
Jurnal Akta Kimia Indonesia (Indonesia Chimica Acta) Volume 1 No 1 - December 2008
Publisher : Hasanuddin University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20956/ica.v1i1.2450

Abstract

The preparation of iron oxide-montmorillonite composite has been done by intercalation of iron oxide into the silicates interlayer of montmorillonite. Montmorillonite and iron oxide-montmorillonite composite were characterized to observe some physical and chemical properties. The observed properties were basal spacing d001, determined by X-Rays Difractometer (XRD); surface morphology, analyzed by SEM/EDAX; specific surface area, distribution of pore radius and total pore volume, analyzed by Gas Sorption Analyzer; functional groups, analyzed by FTIR Spectrophotometer; and iron content, determined by X-Ray Fluorescent Analyzer (XRF). The characterization of montmorillonite and iron oxide-montmorillonite composite showed that the basal spacing d001, increased from 14.11 Å in montmorillonite to 16.85 Å in iron oxide-montmorillonite. Surface morphology of montmorillonite showed the laminated structure, while that of iron oxide-montmorillonite indicated a delaminated structure with the external oxides layered. Specific surface area increased from 69.71 m2/g to 126. 49 m2/g; total pore volume also increased from 50.70 x10-3 mL/g to 107.89 x10-3 mL/g. Generally, spectrum adsorption of montmorillonite and iron oxide-montmorillonite composite not different so far, stretching vibration O-H with Fe3+ does not exist on iron oxide-montmorillonite composite. The iron content also increased from 4.57 %(w/w) to 23.61 %(w/w).Keywords : montmorillonite clay, intercalation, iron oxide-montmorillonit composite.
Co-Authors Candra Y. Tahya Catherina M. Bijang Delvika R. Reawaruw Hanoch J Sohilait Hellna Tehubijuluw Isabella C. Lefmanut Ivonne Telussa J. A. Koritelu Jolantje Latupeirissa Karna Wijaya Matheis F.J.D.P. Tanasale Nurani Hasanela Nurul Ikhsan Rosalina Johannes Triyono .