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All Journal Bulletin of Chemical Reaction Engineering & Catalysis Bulletin of Chemical Reaction Engineering & Catalysis
Herawati Oktavianty
Department of Chemical Engineering, Diponegoro University
Chemical Engineering, Chemistry & Bioengineering Chemistry

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Basicity Optimization of KF/Ca-MgO Catalyst using Impregnation Method Didi Dwi Anggoro; Luqman Buchori; Setia Budi Sasongko; Herawati Oktavianty
Bulletin of Chemical Reaction Engineering & Catalysis 2019: BCREC Volume 14 Issue 3 Year 2019 (December 2019)
Publisher : Department of Chemical Engineering - Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (2323.229 KB) | DOI: 10.9767/bcrec.14.3.4248.678-682

Abstract

This research aimed at determining the optimum value between calcination temperature (X1), calcination time (X2) and %wt KF (X3) toward optimum basicity of KF/Ca-MgO catalyst. Approximately 2-4%wt KF was added to the KF/Ca-MgO catalyst using the impregnation method to assist the Ca-MgO, at 450-550 ºC and a calcination time of 2-4 hours. Furthermore, its basicity was analyzed using Tanabe's titration method. The use of Variance Analysis (ANOVA), indicated that calcination temperature (X1) factor achieved the highest basicity of KF/Ca-MgO catalyst, as indicated by its high F-value (16.46262) and low p-value (0.0067). The correlation between each operating variables and the responses were shown in a mathematical equation. The optimization value is estimated by limiting the calcination temperature from 415.9 to 584.1 ºC, with a calcination time ranging from 1.32 to 4.68 hours, and %wt KF of 1.3182 to 4.6818 % that obtained 1.18 mmol/g for the optimal catalyst basicity. 
Basicity Optimization of KF/Ca-MgO Catalyst using Impregnation Method Didi Dwi Anggoro; Luqman Buchori; Setia Budi Sasongko; Herawati Oktavianty
Bulletin of Chemical Reaction Engineering & Catalysis 2019: BCREC Volume 14 Issue 3 Year 2019 (December 2019)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.14.3.4248.678-682

Abstract

This research aimed at determining the optimum value between calcination temperature (X1), calcination time (X2) and %wt KF (X3) toward optimum basicity of KF/Ca-MgO catalyst. Approximately 2-4%wt KF was added to the KF/Ca-MgO catalyst using the impregnation method to assist the Ca-MgO, at 450-550 ºC and a calcination time of 2-4 hours. Furthermore, its basicity was analyzed using Tanabe's titration method. The use of Variance Analysis (ANOVA), indicated that calcination temperature (X1) factor achieved the highest basicity of KF/Ca-MgO catalyst, as indicated by its high F-value (16.46262) and low p-value (0.0067). The correlation between each operating variables and the responses were shown in a mathematical equation. The optimization value is estimated by limiting the calcination temperature from 415.9 to 584.1 ºC, with a calcination time ranging from 1.32 to 4.68 hours, and %wt KF of 1.3182 to 4.6818 % that obtained 1.18 mmol/g for the optimal catalyst basicity. 
Co-Authors Didi Dwi Anggoro Luqman Buchori Setia Budi Sasongko