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Sintesis dan Karakteristik CaCO3 dari Cangkang Kerang Kepah (Polymesoda erosa) sebagai Doping Anoda Baterai Lithium-Ion Yunior Trisakti; Lizia Miratsi; Widodo Budi Kurniawan
Jurnal Riset Fisika Indonesia Vol 3 No 1 (2022): Desember 2022
Publisher : Jurusan Fisika, Universitas Bangka Belitung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33019/jrfi.v3i1.3548

Abstract

Synthesis and Characteristics of CaCO3 from Kepah Clam Shells (Polymesoda erosa) as Anode Doping of Lithium-Ion Batteries LTO (Lithium Titanate Oxide) or Li4Ti5O12 is one of the candidates for graphite replacement anode material in the production of Lithium-ion batteries. However, LTO materials have the disadvantage of low electrical conductivity, which limits the working level of the battery. Kepah clam shells are one of the wastes that have not been widely used even though the amount is still very abundant, and is expected to have the potential to be in the source of CaCO3 because it contains high amounts of calcium. Therefore, this study aims to determine the content of CaCO3 in the shell of the kepah clam (Polymesoda erosa) and determine the conductivity value of the LTO anode doped with CaCO3 of the kepah clam shell. The synthesis method used is the solid state reaction method with variations in doping concentrations of 0.00 mol, 0.10 mol, 0.15 mol, and 0.20 mol. The results of XRF analysis on the shell powder showed that the most dominant element content was Ca which was 97.63%. So it shows that calcium carbonate (CaCO3) from the shells of kepah mussels was successfully prepared. Furthermore, the anode active material was obtained, which if obtained XRD results and analyzed would show the absence of the CaCO3 phase, and there was no doping influence, then the active material powder was synthesized Li4Ti5O12 anode sheet doped CaCO3 shell. As for knowing the conductivity value of the Li4Ti5O12 anode sheet doped by CaCO3 clam shells, it is further characterized using Electrochemical Impedance Spectroscopy (EIS).
Sintesis Teori A dan B sebagai Upaya Menjelaskan Inonsistensi Teori C dalam Proses Agitated Leaching Tailing Timah Muhammad Sahroni; Anisa Indriawati; Widodo Budi Kurniawan
Jurnal Riset Fisika Indonesia Vol 3 No 2 (2023): Juni 2023
Publisher : Jurusan Fisika, Universitas Bangka Belitung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33019/jrfi.v3i2.4125

Abstract

Inkonsistensi teori C merupakan anomali dimana teori C tidak berlaku dalam proses Agitated Leaching. Hal ini menuntut penjelasan sehingga banyak peneliti berspekulasi untuk menjelaskannya. Contohnya teori A yang kontra- intuitif dan teori B yang cenderung menentang teori A. Dalam penelitian ini telah dilakukan penyelidikan terhadap teori A dan B melalui pendekatan tidak-langsung dengan variabel terikat dari proses Agitated Leaching adalah Total Dissolved Solid (TDS), laju pengadukan sebagai variabel bebas dan variabel tetap adalah rasio solid-likuid (1:20 Gr/mL) dan lama pengadukan (10 menit). Proses pelaruran dilakukan pada keadaan STP dan membatasi proses hanya pada tahap pelarutan sampel menggunakan HNO3 5%. Sampel yang digunakan adalah pasir tailing timah. Hasil penelitian menunjukkan bahwa inkonsistensi terjadi pada laju pengadukan 1000 rpm. Teori A1 tidak dapat disimpulkan keberlakuannya dalam proses pelindian tailing timah. Teori A2 berlaku dalam proses pelindian tailing timah. Teori B berlaku dalam proses pelindian tailing timah.
The Potential of Pepper Shell (Piper Nigrum) for Supercapacitor Electrodes Widodo Budi Kurniawan; Anisa Indriawati; Dewi Marina; Erman Taer
Jurnal Ilmiah Pendidikan Fisika Al-Biruni Vol 8, No 1 (2019): Jurnal Ilmiah pendidikan Fisika Al-Biruni
Publisher : Universitas Islam Negeri Raden Intan Lampung, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24042/jipfalbiruni.v8i1.3780

Abstract

A study has been carried out on supercapacitor electrodes as an electrical energy storage media based on pepper shell activated carbon. The Synthesis is done by mixing the waste carbon pepper shell with an activator HCl with a ratio of 1 : 4. Furthermore, the activated carbon is activated physically by using a pyrolysis temperature of 600 0C. The SEM results indicate that carbon has a porous morphology with a pore size of 24.6 nm which is a mesoporous category. Electrochemical properties are analyzed using cyclic voltammetry (CV). The CV results at the scan rate of 1 mV/s indicate the specific capacitance value generated is 0.45 Fg-1. The results showed that pepper shell waste has the potential to be used as a supercapacitor electrode material
Pengaruh Penambahan Karbon Aktif Dari Kulit Lada dan Suhu Aktivasi Karbon terhadap Nilai Konduktivitas Anoda Berbasis LTO Jefri Akbar; Widodo Budi Kurniawan; Yekti Widyaningrum; Anisa Indriawati
Jurnal Riset Fisika Indonesia Vol 4 No 1 (2023): Desember 2023
Publisher : Jurusan Fisika, Universitas Bangka Belitung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33019/jrfi.v4i1.3823

Abstract

Sintesis dan karakteristik nanopartikel CaO dari cangkang kerang darah (Anadara granosa) menggunakan metode kopresipitasi Nur Hayati; Widodo Budi Kurniawan; Indah Puspita
Jurnal Riset Fisika Indonesia Vol 4 No 2 (2024): Juni 2024
Publisher : Jurusan Fisika, Universitas Bangka Belitung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33019/jrfi.v4i2.4378

Abstract

The lithium ion battery is a type of secondary battery. A good component to be used as the anode of a lithium ion battery is Li4Ti5O12 (LTO). LTO has a low conductivity value so doping is necessary. Doping particle size greatly affects the conductivity of LTO. The purpose of this doping was carried out to find out how the effect of CaO nanoparticle doping on the conductivity value of the LTO battery anode using the coprecipitation method by varying the molarity of NaOH, namely 1M, 3M and 7M. Based on the results of research on the influence of NaOH molarity, it produces different sizes of nanoparticles. The smallest nanoparticle size was obtained in the 3M sample variation, which was 175.0 nm. With a purity of CaO nanoparticles of 96.35%. While the conductivity value of the lithium ion battery doped with CaO nanoparticles with three variations of NaOH molarity, the optimum value was obtained in the 1M sample, which was 1.06 × 10-6 S/cm. This is because the 1M variation produces very low impurities compared to the 3M and 7M variations which have more impurities, this can affect the conductivity value.
Kajian Variasi Massa Karbon Aktif dan Waktu Kontak terhadap Kinetika Adsorpsi Ion Logam Besi (Fe) pada Limbah Cair Batik Cual Rena Aprilianti; Herman Aldila; Widodo Budi Kurniawan
Jurnal Riset Fisika Indonesia Vol 4 No 2 (2024): Juni 2024
Publisher : Jurusan Fisika, Universitas Bangka Belitung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33019/jrfi.v4i2.4416

Abstract

Cual batik liquid waste discharged directly into the environment can cause environmental problems due to containing various heavy metals such as iron metal (Fe). Adsorption method is one of the efforts to reduce heavy metal content in wastewater. This study utilises activated carbon from coconut shell waste to be used as a heavy metal adsorbent. The activated carbon used is the result of physical and chemical activation processes. Based on SEM results, activated carbon has pores with a pore diameter of 81.84 µm and a surface area of 0.2315 cc/g. The adsorption process was carried out using activated activated carbon with mass variations of 0.25 grams, 1.5 grams, and 1.75 grams. Meanwhile, the contact time variations used were 0, 40, 80, 120, and 160 minutes. The results showed that the most optimum mass variation of activated carbon to absorb Fe metal was 1.5 grams with a contact time of 80 minutes which left a residual Fe metal of 0.161 ppm.