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Hidayatulloh, Irwan
Department Of Chemical Engineering, Politeknik Negeri Bandung, Jl. Gegerkalong Hilir, Ciwaruga, Bandung Barat, Jawa Barat 40559, Indonesia
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Proses Pembuatan Minyak Kelapa Murni dengan Menggunakan Rhizopus Oligosporus Moehady, Bintang Iwhan; Hidayatulloh, Irwan
METANA Vol 16, No 1 (2020): Juni 2020
Publisher : Universitas Diponegoro

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (278.604 KB) | DOI: 10.14710/metana.v16i1.25948

Abstract

Minyak kelapa murni merupakan bahan makanan yang banyak digunakan sebagai bahan konsumsi dan bahan tambahan untuk proses industri. Minyak kelapa murni diproduksi dari bahan baku krim santan yang merupakan hasil pelindihan antara air dengan buah kelapa. Pemecahan emulsi pada santan menggunakan teknik ekstraksi kering (dry extraction) dan teknik ekstraksi basah (wet extraction). Penelitian yang dilakukan menggunakan proses ekstraksi basah, yaitu secara fermentasi menggunakan inokulum padat berupa mikroba atau ragi yang dikembangkan pada media padat. Proses tersebut dipilih untuk menyesuaikan dengan situasi masyarakat daerah di Indonesia yang banyak menghasilkan kelapa serta menyesuaikan dengan keberadaan ragi tempe yang telah memasyarakat. Tujuan penelitian ini adalah untuk mendapatkan minyak kelapa dari bahan baku santan (coconut milk) dengan menggunakan inokulum ragi tempe yang mengandung Rhizopus oligosporus. Hasil minyak kelapa murni akan dianalisa parameternya berdasarkan Standar Nasional Indonesia. Dari data percobaan di peroleh hasil analisa produk minyak kelapa murni yang paling optimum sesuai dengan SNI adalah percobaan pada variasi jumlah ragi tempe 0.5 gram dengan jumlah minyak yang dihasilkan 91.35 gram dan nilai kekeruhan 1,8 NTU. Hasil analisis kimia dan fisik: Indeks bias: 1,451, Kadar air: 0,3%, Kadar kotoran: 0,023%, Kadar bebas asam lemak: 0,96%, Kadar minyak Pelikan: 1,82%, angka saponifikasi: 262,969 mgKOH / g lemak. Virgin coconut oil is a food ingredient that is widely used as a consumption material and as an additive for industrial processes. The oil produced from coconut milk cream which was the result of leaching between water and coconut. The emulsion in coconut milk then broken by dry extraction method and wet extraction method. In this research the method carried out by a wet extraction process, which used fermentation using microbes or yeast that was developed on solid media. This process was chosen to adapt to the Indonesian people who produced ton coconut each year and in the same time, the tempeh yeast that has been popular in Indonesia. The purpose of this study was to obtain virgin coconut oil from coconut milk using yeast inoculum containing Rhizopus oligosporus. The parameters of virgin coconut oil analyzed based on the Indonesian National Standard (SNI). The experimental data obtained from the results of the most optimal analysis of virgin coconut oil in accordance with SNI experiments on the variation of the amount of tempeh yeast 0.5 grams with the amount of oil produced 91.35 grams and turbidity value 1.8 NTU. Chemical and physical analysis results: Refractive index: 1,451, Air content: 0,3%, Dirt content: 0,023%, Free fatty acid level: 0,96%, Pelicans oil content: 1,82%, saponification rate: 262,969 mg KOH /g fat.
Aktivitas Bacillus subtilis pada Media Tulang Ayam dalam Pembentukan Gelatin Sudrajat Harris Abdulloh; Bintang Iwhan Moehady; Irwan Hidayatulloh
Fluida Vol 13 No 1 (2020): FLUIDA
Publisher : Jurusan Teknik Kimia, Politeknik Negeri Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35313/fluida.v13i1.2221

Abstract

ABSTRAK Gelatin merupakan bahan tambahan yang banyak terdapat pada industri makanan, minuman, dan tekstil. Gelatin terbentuk secara kimia melalui proses asam dan basa atau dengan bantuan aktivitas mikroorganisme. Proses kimia pembentukan gelatin membutuhkan waktu antara satu sampai lima minggu, sedangkan proses dengan aktivitas mikroorganisme terbentuk antara 12 sampai 24 jam. Penelitian ini bertujuan untuk membuat gelatin dengan menggunakan bakteri Bacillus subtilis ATCC No. 21228 serta bahan baku tulang ayam. Aktivitas bakteri Bacillus subtilis akan merombak kolagen dalam tulang ayam menjadi gelatin. Kondisi operasi yang digunakan yaitu: temperatur 45, 50, dan 55°C; pH 7, 8, dan 9; dan konsentrasi 120 g/L, 160 g/L, 200 g/L dan 240 g/1. Analisis terhadap produk yang diperoleh menggunakan uji kandungan protein dan uji pembentukan gelatin. Hasil penelitian menunjukkan kondisi optimum terjadi pada pH = 9, T = 45°C, konsentrasi (C) = 200 g/L, dan konversi rata-rata = 72,25%. Kata kunci: Gelatin, Bacillus subtilis, limbah tulang ayam ABSTRACT Gelatin is an additive that is widely available in the food, beverage, and textile industries. It is formed chemically through acid and alkaline processes or with the help of microorganism activity. The chemical process for gelatin takes 1-5 weeks, while the process with microorganism activity occur only 12-24 hours. This study aims to make gelatin using the bacteria Bacillus subtilis ATCC No.21228 from raw material for chicken bones. The activity of the Bacillus subtilis bacteria will convert collagen in chicken bones into gelatin. The operating conditions used in this work were: temperature under 45, 50, and 55°C; pH between 7, 8, and 9; and concentrations of 120 g/L, 160 g/L, 200 g/L and 240 gr/1. The result tested to obtain the existing protein and gelatin content. The results showed that the optimum conditions occurred at pH = 9, T = 45°C, concentration = 200 g/L, and the average conversion = 72.25%. Keywords: Gelatin, Bacillus subtilis, chicken bone waste
Kinerja Biakan Murni Rhizopus oligosporus pada Pembuatan Minyak Kelapa Murni (VCO) Irwan Hidayatulloh; Bintang Iwhan Moehady
Fluida Vol 13 No 2 (2020): FLUIDA
Publisher : Jurusan Teknik Kimia, Politeknik Negeri Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35313/fluida.v13i2.2265

Abstract

ABSTRAK Pembuatan minyak kelapa murni dari santan kelapa dapat terjadi oleh perlakuan mikroorganisme yang menyebabkan pecahnya emulsi santan. Penelitian ini bertujuan untuk mendapatkan minyak kelapa dengan menggunakan biakan murni Rhizopus oligosporus dalam bentuk sel bebas pada kondisi optimum temperatur dari mikroba tersebut secara fermentasi batch. Percobaan dilakukan dengan memvariasikan jumlah biakan murni Rhizopus oligosporus. Dari penelitian ini diperoleh hasil VCO terbaik yakni pada percobaan dengan jumlah ragi biakan murni 1.350.000 mikroba/ml pada temperatur 37oC yang menghasilkan produk minyak 81,80 gram. Secara analisis fisik diperoleh turbiditas 3,4 NTU serta warna, bau dan rasa yang normal, sedangkan berdasarkan hasil analisis kimia produk tersebut memiliki kadar air 0,2 %, kadar asam lemak bebas 0,52 % , dan bilangan penyabunan 262,968 mg KOH/g lemak. Kata kunci: Minyak kelapa murni, Rhizopus oligosporus, biakan murni. ABSTRACT The production of virgin coconut oil from coconut milk can be done by microorganism treatment that causes the coconut emulsion to break. This study aims to obtain coconut oil using pure cultures of Rhizopus oligosporus in the form of free cells at optimal temperature conditions of these microbes by batch fermentation. Experiments were carried out by varying the number of pure cultures of Rhizopus oligosporus. From this research, the best VCO result was the experiment done with the amount of pure culture yeast of 1,350,000 microbes/ml at 37oC, producing 81.80 grams of oil product. Physical analysis resulted in turbidity of 3.4 NTU and normal color, odor, and taste, whereas chemical analysis resulted in moisture content of the product of 0.2%, free fatty acid content of 0.52%, and saponification number of 262.968 mg KOH/g fat. Keywords: Pure coconut oil, Rhizopus oligosporus, pure culture
Kajian Pustaka Sintesis Nanoselulosa dari Tandan Kosong Kelapa Sawit sebagai Filler Pembuatan Tisu Toilet Irwan Hidayatulloh; Emmanuela Maria Widyanti; Chandra Aztaris; Awalum Melanitria; Lidya Elizabeth
Fluida Vol 15 No 1 (2022): FLUIDA
Publisher : Jurusan Teknik Kimia, Politeknik Negeri Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35313/fluida.v15i1.2711

Abstract

Tisu merupakan salah satu jenis kertas yang terbuat dari serat kayu. Peningkatan kebutuhan tisu di masyarakat meningkatkan penebangan pohon. Tandan kosong kelapa sawit (TKKS) merupakan limbah dari kelapa sawit yang mengandung selulosa tinggi dan memiliki potensi untuk dimanfaatkan sebagai filler dalam pembuatan tisu. Penelaahan kajian pustaka ini dilakukan untuk mengetahui potensi pemanfaatan nanoselulosa TKKS sebagai filler pembuatan tisu toilet. Sesuai persyaratan, bahan untuk tisu diharapkan mempunyai kandungan selulosa 70 %. Perhitungan kadar selulosa optimum dengan delignifikasi ditentukan dari regresi linear menggunakan software SPSS Statistics 25. Rancangan variabel proses menggunakan software Minitab 19. Metode perancangan yang digunakan dalam percobaan adalah placket burman. Hasil delignifikasi optimum didapatkan pada suhu 150-160°C, NaOH 15-17,5%, dan waktu 20-40 menit. Ukuran diameter nanoselulosa terkecil sebesar 5-10 nm, didapatkan dengan proses hidrolisis asam menggunakan H2SO4 30% pada suhu 60°C selama 120 menit. Nanoselulosa dapat digunakan sebagai filler dalam pembuatan tisu toilet, karena dapat menghasilkan rongga yang dapat menyerap molekul air dan meningkatkan kekuatan lapisan kertas. Tissue is a type of paper, made from wood fibers. The elevation of tissue necessity in the society will rise the trees logging. Oil palm empty fruit bunches (OPEFB) is waste from oil palm mill which contains high cellulose and has a lot of potential to be used, one of that is as a filler in the manufacture of tissue. The literature review was conducted to determine the potential utilization of cellulose in OPEFB as a filler in the manufacture of toilet paper. According to the requirements, the material for tissue is expected to have a cellulose content of 70%. Estimation of optimum cellulose content with delignification was determined by linear regression using SPSS Statistics 25 software. The optimum delignification results were obtained at a temperature of 150-1600C, NaOH 15-17.5%, and 20-40 minutes. The lowest diameter of nanocellulose is 5-10 nm, obtained by acid hydrolysis using 30% H2SO4 at 600C for 120 minutes. The nanocellulose is used as a filler in the manufacture of toilet paper, because it can produce holes that can absorb water molecules and increase the strength of the paper layer.
Nanocellulose Production from Empty Palm Oil Fruit Bunches (EPOFB) Using Hydrolysis Followed by Freeze Drying Irwan Hidayatulloh; Emmanuela Maria Widyanti; Endang Kusumawati; Lidya Elizabeth
ASEAN Journal of Chemical Engineering Vol 21, No 1 (2021)
Publisher : Department of Chemical Engineering, Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/ajche.61093

Abstract

Empty palm oil fruit bunches (EPOFB) are lignocellulose which is abundantly available in Indonesia. EPOFB has big potential as raw materials to substitute wood in nanocellulose manufacture. The production of nanocellulose from EOPFB consists of various stages, such as preparation by grinding and sizing, α-cellulose isolation, acid hydrolysis, and freeze-drying. α-cellulose isolate from POEFB through delignification using 17.5% NaOH (w / v) at 80oC for 30 minutes and bleaching using 10% H2O2 (v / v) at 70oC for 15 minutes. The bleached cellulose was then hydrolyzed by acid hydrolysis process using 64% H2SO4 for 45 minutes with temperature variations to determine the effect of temperature on the size of nanocellulose. Obtained nanocellulose then dried with the freeze-drying method at a temperature of 50oC for 6 hours. The nanocellulose morphology was characterized using SEM analysis, and FTIR analysis was done to determine the presence of cellulose and lignin.  The smallest average diameter obtained at 50oC temperature is 86.8 nm with a 51.5 – 66.5 nm distribution range.
Pengaruh Konsentrasi Pemlastis Pada Aplikasi Edible Coating Dari Tepung Pektin Apel Pada Buah Tomat Naura Alfairuzy Quluby; Revani Triananda; Ayu Ratna Permanasari; Irwan Hidayatulloh; Fitria Yulistiani
Fluida Vol 15 No 2 (2022): FLUIDA
Publisher : Jurusan Teknik Kimia, Politeknik Negeri Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35313/fluida.v15i2.4390

Abstract

The edible coating is a protective layer that can regulate the rate of respiration. The purpose of the study is to see the effect of adding a plasticizer to the edible coating application of apple pectin flour on tomatoes. Edible coating was made with 2% apple pectin flour and plasticizers glycerol and sorbitol in concentrations of 0.5 percent, 0.6 percent, 0.7 percent, 0.8 percent, 0.9 percent, and 1 percent (v/v). Plasticizer concentrations of 1 percent glycerol and 0.7 percent sorbitol were found to be optimal. The addition of 1% glycerol resulted in 3.673 percent tomato fruit weight loss with a shelf life of more than 20 days, and the addition of 0.7 percent sorbitol resulted in 5.718 percent tomato fruit weight loss with a shelf life of more than 7 days. The percentage of elongation (2.47 percent and 1.125 percent), tensile strength (17.10 and 6.61 Mpa), water vapor transmission rate (5.955 and 7.070 g/m2/day), and thickness (0.06 mm) of edible coating with 1 percent glycerol and 0.7 percent sorbitol were obtained. The thickness, tensile strength, and water vapor transmission rate all met Japanese Industrial Standards, according to these results.
Uji Coba Biokoagulan dari Selulosa Cangkang Aren Menggunakan Unit Koagulasi, Flokulasi, dan Sedimentasi Secara Kontinyu Endang Kusumawati; Dea Rahmawati; Fera Rahma Vrilian; Irwan Hidayatulloh
Fluida Vol 15 No 2 (2022): FLUIDA
Publisher : Jurusan Teknik Kimia, Politeknik Negeri Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35313/fluida.v15i2.4400

Abstract

Jawa barat merupakan provinsi yang memiliki luas perkebunan aren paling besar di wilayah indonesia yaitu 14.201 ha. Pohon aren menghasilkan produk olahan utama salah satunya kolang kaling. Produk ini menjadi komoditas ekspor ke berbagai negara di dunia. Namun dari hasil produksi kolang kaling tersebut dihasilkan limbah cangkang yang masih memiliki daya guna rendah. Cangkang aren ini memiliki potensi sebagai biokoagulan karena mengandung selulosa yang memiliki gugus fungsi yang mendukung proses koagulasi. Tujuan dari penelitian ini yaitu mengkarakterisasi biokoagulan cangkang aren, menentukan dosis optimum dan pH optimum biokoagulan cangkang aren dan melakukan uji kinerja biokoagulan pada reaktor kontinyu. Dosis optimum koagulan ditentukan dengan memvariasikan dosis pada rentang 200 – 550 mg/L sedangkan pH optimum ditentukan dengan memvariasikan pH pada rentang 6 - 8,5. Air baku yang diolah menggunakan limbah artifisial dengan kekeruhan awal sebesar 100 NTU. Hasil penelitian dengan metode jar test menunjukan dosis terbaik koagulan selulosa cangkang aren yaitu pada dosis 200 mg/L dan pH terbaik pada pH 8,5. Pada pengujian reaktor kontinyu didapat laju alir terbaik pada laju alir umpan 100 L/jam dengan penurunan kekeruhan 58,287% pada titik setelah lamella clarifier dengan penyisihan TSS sebesar 53,57%.
Pengaruh Konsentrasi Gliserol dalam Edible Coating Tepung Biji Nangka dengan Penambahan Plasticizer Gliserol Emmanuela Maria Widyanti; Nancy Siti Djenar; Ari Marlina; Endang Widiastuti; Irwan Hidayatulloh; Intan Puspitarini; Dhara Firdausa; Lidya Elizabeth
Fluida Vol 15 No 2 (2022): FLUIDA
Publisher : Jurusan Teknik Kimia, Politeknik Negeri Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35313/fluida.v15i2.4419

Abstract

Tomatoes are horticultural plants that are easily damaged, need to be coated with a food grade edible coating. The basic ingredients that can be used are polysaccharides, derived from jackfruit seed flour, then glycerol plasticizer is added to improve the brittle nature of the edible coating. The maximum glycerol added was carried out with the following concentration variations: control (without glycerol), 1.5%, 2.0%, 2.5%. The analysis carried out included testing the respiration rate and weight loss in tomato storage for 6 days. In determining the respiration rate, an experiment was carried out by flowing 1 L/minute of air for 2 minutes which had been passed through a saturated Ca(OH)2 solution flowed into a jar containing tomatoes, passing through a 0.05 N NaOH solution added 0.1% phenophthalein indicator and titrated with HCl 0.05 N until the red color disappears and the weight loss decreases on tomatoes coated with edible coating. The results obtained were the lowest decrease in respiration rate at 2% glycerol concentration of 0.137 mgCO2/kg.hour and the lowest decrease in weight loss at 2.5% glycerol concentration of 1.913%.
Kajian Pustaka Sintesis Nanoselulosa dari Tandan Kosong Kelapa Sawit sebagai Filler Pembuatan Tisu Toilet Irwan Hidayatulloh; Emmanuela Maria Widyanti; Chandra Aztaris; Awalum Melanitria; Lidya Elizabeth
Fluida Vol 15 No 1 (2022): FLUIDA
Publisher : Jurusan Teknik Kimia, Politeknik Negeri Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35313/fluida.v15i1.2711

Abstract

Tisu merupakan salah satu jenis kertas yang terbuat dari serat kayu. Peningkatan kebutuhan tisu di masyarakat meningkatkan penebangan pohon. Tandan kosong kelapa sawit (TKKS) merupakan limbah dari kelapa sawit yang mengandung selulosa tinggi dan memiliki potensi untuk dimanfaatkan sebagai filler dalam pembuatan tisu. Penelaahan kajian pustaka ini dilakukan untuk mengetahui potensi pemanfaatan nanoselulosa TKKS sebagai filler pembuatan tisu toilet. Sesuai persyaratan, bahan untuk tisu diharapkan mempunyai kandungan selulosa 70 %. Perhitungan kadar selulosa optimum dengan delignifikasi ditentukan dari regresi linear menggunakan software SPSS Statistics 25. Rancangan variabel proses menggunakan software Minitab 19. Metode perancangan yang digunakan dalam percobaan adalah placket burman. Hasil delignifikasi optimum didapatkan pada suhu 150-160°C, NaOH 15-17,5%, dan waktu 20-40 menit. Ukuran diameter nanoselulosa terkecil sebesar 5-10 nm, didapatkan dengan proses hidrolisis asam menggunakan H2SO4 30% pada suhu 60°C selama 120 menit. Nanoselulosa dapat digunakan sebagai filler dalam pembuatan tisu toilet, karena dapat menghasilkan rongga yang dapat menyerap molekul air dan meningkatkan kekuatan lapisan kertas. Tissue is a type of paper, made from wood fibers. The elevation of tissue necessity in the society will rise the trees logging. Oil palm empty fruit bunches (OPEFB) is waste from oil palm mill which contains high cellulose and has a lot of potential to be used, one of that is as a filler in the manufacture of tissue. The literature review was conducted to determine the potential utilization of cellulose in OPEFB as a filler in the manufacture of toilet paper. According to the requirements, the material for tissue is expected to have a cellulose content of 70%. Estimation of optimum cellulose content with delignification was determined by linear regression using SPSS Statistics 25 software. The optimum delignification results were obtained at a temperature of 150-1600C, NaOH 15-17.5%, and 20-40 minutes. The lowest diameter of nanocellulose is 5-10 nm, obtained by acid hydrolysis using 30% H2SO4 at 600C for 120 minutes. The nanocellulose is used as a filler in the manufacture of toilet paper, because it can produce holes that can absorb water molecules and increase the strength of the paper layer.
The Effect of Maltodextrin Concentration and Spray Dryer Drying Temperature on the Characteristics of Coconut Milk Powder Fitria Yulistiani; Alifia Nuraeni; Sheilla Aulia Sofiatul Mardiah; Irwan Hidayatulloh; Lidya Elizabeth; Nurcahyo
Fluida Vol 16 No 1 (2023): FLUIDA
Publisher : Jurusan Teknik Kimia, Politeknik Negeri Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35313/fluida.v16i1.4006

Abstract

Coconut milk has a higher water content than other contents, so microbes can easily damage and spoil it. To obtain a low-moisture powder product, the liquid coconut milk was dried using a Buchi Mini Spray dryer B-290 with inlet temperatures of 150°C, 160°C, and 170°C. The researchers added maltodextrin to coconut milk, which had a ratio of grated coconut to the water of 1:3, in concentrations of 9%, 10%, 11%, 12%, and 13%. The addition of maltodextrin and the use of drying temperature did not significantly affect the pH, solubility, and percentage of product mass but did significantly affect the moisture content. The best operating conditions for producing coconut milk powder were at a maltodextrin concentration of 13% and a temperature of 170°C. Under these conditions, the produced coconut milk powder had a pH value of 6.12, a moisture content of 4.56%, a solubility of 98.74%, a product mass of 24.99 grams and an overall percentage of product mass of 21.32%.
Co-Authors Alifia Nuraeni Ari Marlina Awalum Melanitria Bintang Iwhan Moehady Bintang Iwhan Moehady Chandra Aztaris Dea Rahmawati Dhara Firdausa Endang Kusumawati Fera Rahma Vrilian Intan Puspitarini Lidya Elizabeth Mira Rachmawati Syabila Moehady, Bintang Iwhan Nancy Siti Djenar Naura Alfairuzy Quluby Nurcahyo Permanasari, Ayu Ratna Pipit Febrianti Revani Triananda Sheilla Aulia Sofiatul Mardiah Sudrajat Harris Abdulloh Widiastuti, Endang Widyanti, Emmanuela Maria Yulistiani, Fitria