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Journal : Indonesian Review of Physics (IRiP)

Characterization of Activated Charcoal Oil Palm (Elaeis Guineensiss Jacq) Shell Waste using SEM and FTIR: Effect of Activation Temperature Rasyid Syidiq; La Ode Yusran; Muhammad Anas; Suritno Fayanto
Indonesian Review of Physics (IRiP) Vol. 2 No. 2 (2019)
Publisher : Universitas Ahmad Dahlan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.12928/irip.v2i2.812

Abstract

This study aims to determine the structure of morphology and functional groups from activated charcoal for palm oil waste with variations in activation temperature. The process of two stages: the carbonation and activation stage. Carbonation process using a pyrolysis reactor at a carbonation temperature of 200oC -400oC for 6 hours. Then, the sample activated at a temperature of 700 °C, 750oC, 800oC, and 850 °C. Samples were characterization using SEM and FTIR. SEM analysis results show the largest pore size at a temperature of 850 oC with a diameter of 48.3 nm, and the lowest temperature was 700 °C with a capacity of 35.3 nm. Activated charcoal from oil palm shell waste at mesopore size. Next, FTIR analysis results show wave numbers 2165,18 cm-1, 1554 cm-1, 1030,76 cm-1 dan 424,11 cm-1.  The removal of some absorption bands and  the formation of new absorption bands, caused by the activation temperature
Investigating The Effects of Activation Temperature on The Crystal Structure of Activated Charcoal From Palm Bunches (Arengga Pinnata Merr.) Vivi Hastuti Rufa Mongkito; Muhammad Anas; Wisda Puspita Bahar
Indonesian Review of Physics (IRiP) Vol. 2 No. 1 (2019)
Publisher : Universitas Ahmad Dahlan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.12928/irip.v2i1.818

Abstract

This research aims to determine the effect of activation temperature the crystal structure of activated charcoal. The material used activated charcoal bunches (Arengga Pinnate Merr). The process of making activated charcoal divided into two, namely the carbonization stage at a temperature of 250- 400 oC and the activation stage at a temperature variation of 600 - 800 ÌŠC. To find the crystal structure, the sample characterized by X-Ray Diffraction. The results of analysis the dominant elements diamond before activation with a percentage of 90.2% and an orthorhombic crystalline structure, where the lattice parameter a = 4.12700 Ã…; b = 4.93700 Ã…; c = 4.81900 Ã…. Peak Carbon has a hexagonal crystal structure in all temperature variations. Peak Graphite an orthorhombic crystal structure and at a temperature of 700 oC a hexagonal crystal structure formed. Therefore, giving temperature variations the activated charcoal of the bunches affects the structure of the formed Crystal. Wherein increasing the activation temperature, the crystal structure that forms look more amorphous marked by a widening diffraction peak intensity decreased crystals