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All Journal Jurnal Penelitian Hasil Hutan Jurnal Pendidikan Kimia (JPKim) Jurnal Penelitian Hasil Hutan

Ibrahim, Agus Malik

Sekolah Tinggi Analis Kimia Cilegon, Cilegon, Banten, Indonesia

Author-ID : 3951370

Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Decision Sciences, Operations Research & Management Education Energy Environmental Science Materials Science & Nanotechnology

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Analysis of secondary metabolite compounds from leaves extract kesambi (Schleichera oleosa) and antioxidant activity test Boima Situmeang; Weny Nuraeni; Agus Malik Ibrahim; Saronom Silaban
Jurnal Pendidikan Kimia (JPKim) Vol 8, No 3 (2016): Desember
Publisher : Pascasarjana Universitas Negeri Medan

Abstract. Kesambi (Schleichera oleosa) is one of plants that have the potential to treat various deasease. Kesambi plant or kusum widely spread in Asia such as India, Nepal, Malaysia and Indonesia. In Indonesia, this plant widely available in Java precisely Cilegon and Jember area. This study aimed to analyze the content of secondary metabolites from plants kesambi extract and antioxidant activity test of hexane, ethyl acetate and water fraction. Analysis of secondary metabolites is done with phytochemical and GC-MS test methods. Extraction was done by using maceration and fractionation methods. Antioxidan tactivity test using DPPH methods. The content of secondary metabolites contained in leaves kesambi (Schleichera oleosa) are flavonoids, alkaloids, tannins, phenols, and steroids. Based on IC50 values were obtained from three fraction, ethyl acetate fraction had a strong radical inhibition rate than the fraction of water and n-hexane. IC50 fraction of ethyl acetate, water, and n-hexane successively are: 206.0851; 272.2891 and 425,1143 ppm respectively. Keyword: kesambi, schleichera oleosa, DPPH, antioxidant

Synthesis and characterization of capsule shells non gelatin grass jelly leaves-seaweed as drug delivery system material Micha Mahardika; Fauzan Amin; Ika Agustia Umami; Boima Situmeang; Agus Malik Ibrahim
Jurnal Pendidikan Kimia (JPKim) Vol 13, No 1 (2021): April
Publisher : Pascasarjana Universitas Negeri Medan

Drug delivery system is a system that describes the journey of a drug to its target location. The main component of the drug delivery system is gelatin. The leaves of grass jelly-seaweed are needed as a raw material for gelatin. The main component of gelling agents in grass jelly leaves and seaweed is a low-methoxy pectin polysaccharide. Pectin from previous study is used as a synthesis material for hard capsule shells with the addition of other ingredients, which are Na-CMC, sorbitol, and water. The characterization results of capsule shells with variations in the composition of grass jelly-seaweed leaves 0: 4, 1: 3, 2: 2, 3: 1, and 4: 0 (A, B, C, D and E) have a disolving time of 12 minutes 45 seconds; 15 minutes 53 seconds; 23 minutes 10 seconds; 15 minutes 35 seconds and 18 minutes 12 seconds. The swelling degree test each of 200%; 266,7%; 303.3%; 586.7% and 643.3%. Furthermore, the shells of grass jelly-seaweed leaf capsules were tested for their material performance in the cefadroxyl disolving test with variations in sampling time of 10, 20, and 30 minutes.Keywords: Cefadroxyl, Drug delivery system, Green grass jelly leaves, Non-gelatin capsules, Seaweed

Utilization of leaf and fruit extracts of kedondong (Spondias dulcis Forst) as a supporting material for energy conversion in dye sensitized solar cells and electrochemical cells Agus Malik Ibrahim; Boima Situmeang; Ahmad Rifa’i; Afif Hidayatul Mustafid
Jurnal Pendidikan Kimia (JPKim) Vol 13, No 1 (2021): April
Publisher : Pascasarjana Universitas Negeri Medan

This study aims to obtain a dye sensitized solar cell (DSSC) prototype and a voltaic cell prototype using the kedondong plant (Spondias dulcis Forst). Kedondong leaves as a source of chlorophyll were deliberately chosen to be in line with the use of kedondong fruit as a material for electrochemical cells, so that two research results could be obtained from the kedondong plant. This research is for the application of scientific development, increasing the added value of kedondong plant, and as support for the use of environmentally friendly energy. Research methods in general are chlorophyll extraction, citric acid isolation, chlorophyll testing, DSSC assembly, electrochemical cell assembly, and performance testing for both DSSC and electrochemical cells. The analysis results show that typical peaks appear for the functional groups in chlorophyll at certain wave numbers. Hydroxyl (-OH) groups appear in the range of 3650 - 3200 cm-1, the C=C group at 1700 - 1500 cm-1, the C-N group at 1350 - 1000 cm-1, and the C-O group at 1300 - 1000 cm-1. Quantitative testing used a UV-Vis spectrophotometer at 645 nm and 633 nm, the results obtained were chlorophyll a was 4.52 mg/L, chlorophyll b was 8.43 mg/L, and total chlorophyll was 12.95 mg/L. The DSSC prototype performance test with a size of only 2.5 cm2, can produce a minimum voltage of 30.1 mV and a maximum of 280 mV. The electrochemical test of kedondong citric acid extract showed that the value of the electric voltage ranged from 121 to 630 mV.Keywords: Kedondong, Chlorophyll, DSSC, Citric acid, Electrochemical cells

Antibacterial activity and phytochemical screening of Kesambi (Sapindaceae) against Eschericia coli and Staphylococcus aureus Boima Situmeang; Agus Malik Ibrahim; Nurhayati Bialangi; Weny J.A Musa; Saronom Silaban
Jurnal Pendidikan Kimia (JPKim) Vol 11, No 1 (2019): April
Publisher : Pascasarjana Universitas Negeri Medan

Kesambi plant (Schleichera oleosa) is a medicinal plant belongs to family Sapindaceae, commonly found in tropical and subtropical regions of the world. In Indonesia, kesambi plants can be found in Java and Bali island. The purpose of this study is to extraction and antibacterial activity test of steam bark extract of kesambi against Escherichia coli and Staphylococcus aureus. Extraction was done by maceration method using n-hexane, ethyl acetate and methanol. Antibacerial test using Kirby bauer method by measure inhibition zone. Phytochemical screening shown that n-hexane extract contain triterpenes and steroid compounds. Ethyl acetate extract contain triterpenes, flavonoid, steroid, and fenolic compounds. Methanol extract contain flavonoid, fenolic and triterpenes compounds. Inhibition zone of n-hexane, ethyl acetate and methanol extracts against E. coli and S. aureus at concentration of 5000 µg/mL showed 4.4; 7.9; 4.6 mm and 4.7; 8.9; 4.5 respectively, while amoxicillin and ciprofloxacin as positive control at concentration of 100 µg/mL showed 6.9 and 7.1 mm respectively. Kesambi extract have potential as antibacterial against E. coli and S. aureus.Keywords:Kesambi; antibacterial; Eschericia coli; Staphylococus aureus

Co-Authors Afif Hidayatul Mustafid Agrin Febrian Pradana Ahmad Rifa’i Boima Ramses Situmeang Boima Situmeang Fauzan Amin Gagas Priyosakti Gustan Pari Ika Agustia Umami Irma Herawati Suparto Micha Mahardika Miftahul Arifin Nurhayati Bialangi Perliansyah Perliansyah Saronom Silaban Saronom Silaban Tetty Kemala Tuti Alawiyah Weny J.A Musa Weny Nuraeni

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