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Istiqomah Rahmawati
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Journal of Biobased Chemicals (JOBC)
Published by Universitas Jember
ISSN : 27463257     EISSN : 27462544     DOI : https://doi.org/10.19184/jobc.v2i1.116
Core Subject : Science, Engineering,
Chemical Engineering, Chemistry & Bioengineering Chemistry
The scopes of this journal include the following topics: 1. Components extract from bioresources 2. Chemical and physical processing of biomass 3. Biobased materials and composites 4. Biobased energy production 5. Catalyst technology for biomass conversion 6. Biological processing of bioresources, chemicals and waste 7. Treatment of biobased chemical waste 8. Application of the biobased chemical products to the target users 9. System analysis, management, and environmental protection of biobased chemical processing This journal does not consider the topics about organic chemicals from non-organism, crops and breeding, organism modification, metabolic engineering, bioresources and environmental management which do not relate to biobased chemical processing.
Arjuna Subject : Teknik Kimia (semua kategori) - Bioengineering
Articles 30 Documents
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Effect of Time, pH, and Yeast Concentration on Bioethanol Levels in the Ulva sp. Fermentation Process Aina Christalia Rinastiti; Dianita Ivana Permata; Bekti Palupi; Zuhriah Mumtazah; Meta Fitri Rizkiana; Atiqa Rahmawati
Journal of Biobased Chemicals Vol. 2 No. 2 (2022): Journal of Biobased Chemicals
Publisher : Program Studi Teknik Kimia Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/jobc.v2i2.269

Abstract

Bioethanol is a form of renewable energy that is used to reduce dependence on the use of fossil fuels which cause various negative impacts on the environment. Ulva sp. contains high carbohydrates so it has the potential as a raw material for bioethanol production. This study aims to determine the optimum conditions of the fermentation process with the variables used time, pH, and yeast concentration. This study used the results of hydrolysis of Ulva sp. with optimum operating conditions of 0.1 N HCl concentration, 80 mesh particle size, and 450 watt microwave power. Measurement of bioethanol levels was carried out using an alcoholmeter. The results showed that the optimal conditions for fermentation were 7 days of fermentation, pH 5.5, and yeast concentration of 1.5% which resulted in a bioethanol content of 7.55%.
Extraction Method of Ultrasound-Assisted Extraction (UAE) of Robusta Coffee Skin Waste using 96% Ethanol Solution in Tanah Wulan Village, Maesan District, Bondowoso Regency Miftakhul Ulum; Fitriah Novita Sari; Helda Wika Amini; Hanggara Sudrajat
Journal of Biobased Chemicals Vol. 2 No. 2 (2022): Journal of Biobased Chemicals
Publisher : Program Studi Teknik Kimia Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/jobc.v2i2.270

Abstract

Argopuro Mountains, Tanah Wulan Village, Maesan District, Bondowoso Regency, East Java, Indonesia is one of the Robusta coffee-producing areas. Robusta coffee beans that are processed can produce quite a lot of by-products in the form of underutilized waste. It is known that coffee skin waste still has a lot of remaining content and it is possible to take these bioactive compounds using extraction methods. Bioactive compounds in natural materials can be done by extraction. Extraction is the process of separating substances in a sample based on different solubilities. The extraction method used is the ultrasonication method (nonconventional). Extraction of the ultrasonication method only requires a relatively shorter time with the help of an ultrasonicator. There is a lot of content in the coffee skin waste powder that needs further testing. The results of this study are expected to provide economic value to robusta coffee husk waste.
Effect of Ethanol Solvents in the Extraction Process of Bioactive Compounds from Brown Seaweed (Sargassum sp.) with the Ultrasound Assisted Extraction Method Slamet Pujianto; Boy Arief Fachri; Istiqomah Rahmawati; Erna Subroto
Journal of Biobased Chemicals Vol. 2 No. 2 (2022): Journal of Biobased Chemicals
Publisher : Program Studi Teknik Kimia Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/jobc.v2i2.271

Abstract

Sargassum sp., part of brown algae, is traditionally used as animal feed. Nonetheless, Sargassum contains phenolic compounds that promise to be the raw material of natural antioxidants. The work is to extract phenolic compounds from Sargassum sp. in ethanol and to investigate the effect of the process on phenol yields. Several dried Sargassum sp. are milled in a certain size and extraction using ultrasound assisted extraction with ethanol solvent. Process variables are the extraction time (30-50 minutes) and the Ratio of Sargassum sp. to ethanol which is 5:100-15:100 (b/v), and power of 170-190 watts. Phenol compounds are quantified using the error acid method. The DPPH method is performed to check the antioxidant activity. To investigate the influence of the process, surface response methods based on central composite designs are applied in this work. 153.334 mgGAE/g in 30-minute extraction conditions, 170 watts of power, and a ratio between masses and solvents of 0.05. The antioxidant activity (IC50) of Sargassum sp. extract is 87.57 ppm.
Microwave Assisted Hydrolysis Ulva sp. Using HCl for the Production of Bioethanol Raw Materials Bekti Palupi; Nadia Ayumna Fa’iqoh; Alifia Rahma Putri Neysella; Boy Arief Fachri; Ditta Kharisma Yolanda Putri; Lukman Nulhakim; Maulida Septiyana
Journal of Biobased Chemicals Vol. 2 No. 2 (2022): Journal of Biobased Chemicals
Publisher : Program Studi Teknik Kimia Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/jobc.v2i2.272

Abstract

The challenges faced by the Indonesian state are increasing greenhouse gases, climate change, and depleting fossil fuel reserves. This requires the exploration of alternative energy that is environmentally friendly and sustainable. Algae biomass, especially Ulva sp. is one of the resources that have the potential for bioethanol production as an alternative energy producer. The purpose of this study is to determine the potential of Ulva sp. as raw material for bioethanol and to determine the effect of particle size, solvent concentration, and power on the hydrolysis process. This study used Ulva sp. as raw material. hydrolyzed with HCl solvent using the microwave assisted hydrolysis method. Hydrolysis with HCl concentrations of 0.1 N, 1 N, 2 N, variations of microwave power 150 watts, 300 watts, 450 watts, and particle sizes of 60 mesh, 80 mesh, and 100 mesh. Measurement of reducing sugar levels was carried out using the dinitro salicylic acid (DNS) method. The results showed that the best conditions for hydrolysis were when the HCl concentration was 0.1 N, the microwave power was 450 watts, and the particle size was 80 mesh which resulted in a reducing sugar content of 20.751 mg/mL.
Effect of Ethanol Solution Concentration in the Extraction Process of Centella asiatica L. Bioactive Components Using Microwave-Assisted Extraction (MAE) Method Fira Ulvatur Rohmah; Rina Auliyah Safitri; Ayu Ulum Rahmawati; Atiqa Rahmawati
Journal of Biobased Chemicals Vol. 2 No. 2 (2022): Journal of Biobased Chemicals
Publisher : Program Studi Teknik Kimia Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/jobc.v2i2.274

Abstract

The Pegagan plant has a scientific name in the form of Centella asiatica L. which is included in the Centella genus, Apiaceae family, and kingdom Plantae. Pegagan (Centella asiatica L.) has distinctive bioactive components, namely triterpene ester glycoside compounds in the form of asiaticoside and madecassoside, and triterpene group compounds in the form of Asiatic acid and madecassic acid. In this study, the extraction of bioactive components from pegagan was carried out using the Microwave-Assisted Extraction (MAE) method and will study the effect of ethanol solvent concentration in the extraction of bioactive compounds. Analysis of the extracted bioactive content was carried out by analyzing the total phenol content using the Folin-Ciocalteau reagent and ANOVA analysis. The results obtained from the study were in the form of total phenol content as an indication of the presence of bioactive compounds, namely at operating conditions of 450 watts of power, 50% ethanol concentration with a radiation time of 15 minutes which resulted in a total phenol content of 21.9244 mg AGE/g sample. In the ANOVA analysis with ethanol solvent, variables that gave a significant response to the total phenol content were microwave power, radiation time, and ethanol concentration with an R-square value of 95.31%. The effect of ethanol concentration on the total phenol content produced, namely the concentration of pure ethanol solvent will produce extracts with the smallest total phenol content, the effect of extraction time on total phenol content, namely the longer extraction time will increase the total phenol content. Maximum total phenol content using ethanol solvent that is, at operating conditions of 450 watts of power, 10% ethanol concentration with a radiation time of 15 minutes which resulted in a total phenol content of 520 mg AGE/g sample.
Optimasi Uji Total fenolik Labu Siam (Sechium edule) Menggunakan Ultrasonic-Assisted Extraction dan Response Surface Methodology Relyando, Syahfa Adinda; Ayu Wulandari; Ditta Kharisma Yolanda Putri; Bekti Palupi; Istiqomah Rahmawati
Journal of Biobased Chemicals Vol. 3 No. 1 (2023): Journal of Biobased Chemicals
Publisher : Program Studi Teknik Kimia Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/jobc.v3i1.276

Abstract

Chayote (Sechium edule) is a plant from the Cucurbitaceae family that contains several vitamins such as vitamins A, B, and C, and is often used for medicinal purposes. Based on phytochemical analysis, chayote extract contains bioactive compounds in the form of phenolics. Phenolic compounds are secondary metabolites and are used as cosmetic and medicinal ingredients due to their ability to reduce oxidative stress. This research aims to determine the total phenolic content and antioxidant activity of chayote (Sechium edule) extract using UV-Vis spectrophotometry. Chayote extract was obtained using the Ultrasonic Assisted-Extraction (UAE) method with 96% ethanol solvent. The extraction variables used were time (15, 20, and 25 minutes), amplitude (45, 65, and 85%), and solvent ratio (1:5, 1:10, and 1:15). The determination of total phenolic content was based on the Folin-Ciocalteau method, while antioxidant activity was determined using DPPH. The determination of chayote extraction parameters for total phenolic content was carried out using the Response Surface Methodology with a Box-Behnken type. The optimal conditions obtained for chayote extraction were 1.327 mg GAE/g sample for total phenolic content and 29.45% for antioxidant activity under the conditions of 20 minutes extraction time, 65% amplitude, and 1:10 solvent ratio.
Extraction of Phenolic Active Compounds from Coffee Leaves (Coffea sp.) Using the Ultrasound Assisted Extraction Method and Total Phenol Analysis Alfinaini, Nur Aini Dwi Alfinaini; Boy Arief Fachri; Pratamai Shelli; Helda Wika Amini; Istiqomah Rahmawati
Journal of Biobased Chemicals Vol. 3 No. 1 (2023): Journal of Biobased Chemicals
Publisher : Program Studi Teknik Kimia Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/jobc.v3i1.278

Abstract

Coffea sp. is one of the largest plantation commodities in Indonesia, especially coffee leaves containing phenolic compounds. This research was conducted to extract phenolic compounds using the Ultrasound-Assisted Extraction method with ethanol solvent which aims to determine the optimum operating conditions of extraction as well as the influence of variations in amplitude, time, and ratio of solvents produced. The experimental design was carried out using Design Expert 13 software with the response surface method box-Behnken design. The research variables used were amplitude variations (50%, 60%, and 70%), time (10, 20, and 30 minutes), and solvent ratios (0.1; 0.15; and 0.2 g/mL).Based on our study, these parameters affect the total phenolic content. The model equation for the total phenolic content of coffee leaves obtained is Y = 0.1349 – 0.0016 A – 0.0505 B + 0.0010 C + 0.0018 AB + 0.0043 AC – 0.0018 BC – 0.0004 A2 + 0.0178 B2 – 0.0014 C2 (R2 = 0.9758) with the optimum total phenolic content located in the 17th running of 0.209 mg GAE/g under conditions of 20 minutes, the ratio of material to solvent is 0.2 g/mL, and an amplitude of 50%.
Preparation of a hollow fiber membrane made of antifouling PVDF/Zeolit using the dip-coating technique Mumtazah, Zuhriah; Adinda Yufriza; Husna Wardati; Ditta Kharisma Yolanda Putri; Meta Fitri Rizkiana; Reva Edra Nugraha
Journal of Biobased Chemicals Vol. 3 No. 1 (2023): Journal of Biobased Chemicals
Publisher : Program Studi Teknik Kimia Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/jobc.v3i1.279

Abstract

The practical technique for membrane modification is dip coating. This study coats a PVDF hollow fiber membrane-based composite with a coating of zeolite. The composite is made of a polyvinylidene fluoride (PVDF) membrane. During water filtering, the separation capabilities and propensities of composite membranes for organic impurities were examined. Fourier-transform infrared spectroscopy analysis of the findings demonstrated that the Zeolite coating was successfully deposited on the PVDF membrane. The flux recovery ratio increases from 69% to 80% while the relative flux drop decreases from 63% to 50%. A composite PVDF membrane dip-coating of Zeolite with a GA and H2SO4 ratio of 1:2 is needed to remove about 75% of humic compounds from effluent. The results of this study show that the addition of Zeolite with a GA and H2SO4 layer can greatly improve the hydrophilicity, selectivity, and anti-organic fouling of the PVDF hollow fiber membrane.
Efficient Anthocyanin Extraction from Aqueous Mixture of Cocoa Peel Using Microwave Assisted Extraction (MAE) Method Lutsi, Nurtsulutsiyah; Yakub Hendrikson Manurung; Istiqomah Rahmawati
Journal of Biobased Chemicals Vol. 3 No. 1 (2023): Journal of Biobased Chemicals
Publisher : Program Studi Teknik Kimia Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/jobc.v3i1.281

Abstract

Anthocyanins are polyphenolic compounds whose existence is very abundant in nature with diversity in various types of plants. The purpose of this study was to optimize the anthocyanin extraction process from cocoa shell waste using the MAE method in order to obtain the optimum particle size, ingredient/solvent ratio, and extraction time to produce high anthocyanin concentrations. The optimized extraction process variables include the size of the particle (1,05; 1,25; 1,49 and 2,5 x 10-4 m), the ratio of substrate/solvent (4,5; 12,5; 62,5; 79,5 x 10-3 g/mL), time of extraction (2, 4, 10, 14 minutes) and microwave power (100; 275; 450; 625 watts). The Design Expert vs11 program with the Box-Behnken Design Response Surface Methodology (RSM) was used in the research and the selection of process conditions was carried out from a combination of factors that resulted in an optimal response. The relationship between variables on the modeled anthocyanin concentration response: Y=0,000486-9,98637E-07A+0,026734B0,000041C-7,58240E-07D-0,000102AB+2,48606E-07AC+2,62878E09AD-0,000539BC+0,000012BD+9,71853E08CD (A: particle size; B: cocoa shell: solvent ratio; C: extraction time; D: microwave power). The optimal response value for anthocyanin concentration was 11,85.10-4 M and the conditions of the extraction process are the particle size in the extraction process was 0,105 mm, the ratio of cocoa peel mass/ethanol was 0,03125 g/mL, the extraction time was 2 minutes, and the microwave power was 100 W.
Adsorption of Methylene Blue by Magnetic Activated Carbon/Chitosan Composites Prepared from Spent Coffee Grounds : Kinetic, Equilibrium and Thermodynamic Study Santosa, Iliya Kartika; Meta Fitri Rizkiana
Journal of Biobased Chemicals Vol. 3 No. 1 (2023): Journal of Biobased Chemicals
Publisher : Program Studi Teknik Kimia Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/jobc.v3i1.282

Abstract

Spent coffee grounds were used as the main ingredient for the composing of magnetic activated carbon/chitosan (MACC) composites and synthesized using the coprecipitation method. The SEM-EDX characterization was used to understand elemental identification and morphology of the adsorbent before the MACC was applied for the removal of methylene blue (MB) from aqueous solution. Magnetic activated carbon/chitosan was fabricated with the subsequent circumstances: the molar ratio of ferrous/ferric ions was 0.02 mol : 0.01 mol, coprecipitation temperature at 60°C for 5 h. Adsorption parameters for MB were investigated. The adsorption by MACC was evaluated thermodynamically for the discharge of MB from an aqueous solution as adsorption reckon on temperature. Calculations of thermodynamic parameters were conducted. Batch adsorption experiments were operated at 308 K; 318 K and MB concentration of 5-50 mg L-1 to investigate the adsorption behavior. According to the results, MACC has a porous structure. The adsorption process is more reactive upon raising the temperature, a process commonly known as endothermic. Based on R2values, the adsorption of MB onto MACC was found best fitted to Freundlich model. The maximum adsorption capacity of the MACC was counted as 24.5 mg/g. The adsorption process is spontaneous, which was concluded from the calculation of thermodynamic parameters.

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