Claim Missing Document
Check
Articles

Found 1 Documents
Search
Journal : VALENSI

Deconvolution of TEOS/TEVS Xerogel by Single or Dual Organic Catalyst Addition Anna Sumardi; Muthia Elma; Aptar Eka Lestari; Zaini Lambri Assyaifi; Adi Darmawan; Isna Syauqiah; Erdina Lulu Atika Rampun; Yanti Mawaddah; Linda Suci Wati
Jurnal Kimia Valensi Jurnal Kimia VALENSI Volume 6, No. 2, November 2020
Publisher : Syarif Hidayatullah State Islamic University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.15408/jkv.v6i2.17597

Abstract

Currently, xerogel has been applied as a filtration material, especially in membrane desalination. However, the xerogel matrix structure for desalination have to be designed properly in order to allow rejection of salt and obtain good hydro-stability, thus, silica precursor in the form of TEOS (tetraethyl orthosilicate)/TEVS (triethoxy vinyl silane) and organic acid catalyst are suitable material for fabrication. The aim of this study is therefore to fabricate and perform deconvolution of TEOS/TEVS xerogel by adding single or dual catalyst, using FTIR (Fourier-transform Infrared Spectroscopy) and Fityk software. The xerogel was fabricated by dried silica sol and calcined using RTP technique (rapid thermal processing) at 450 °C.  Prior to this fabrication, the silica sol was synthesized by sol gel method, using a mixture of silica precursor TEOS/TEVS, ethanol solvent, and varied addition of single catalyst (citric acid) as well as dual catalyst (citric acid + ammonia) for 2 hours, at 50 °C. Subsequently, the xerogel was characterized by FTIR and the deconvolution was obtained through Gaussian approach, with Fityk software. All TEOS/TEVS xerogel samples indicated existence of silanol (Si-OH), siloxane (Si-O-Si) and silica-carbon (Si-C) functional groups. The xerogel deconvolution of TEOS/TEVS using single catalyst exhibit a peak area ratio of Si-OH/Si-O-Si, and this is similar to the dual catalyst counterpart of 0.24 (unit area) and 1.86 (unit area), for Si-C area ratio. This shows the addition of single catalyst was enough to produce deconvolution in TEOS/TEVS xerogel, dominated by siloxane functional group and carbon bonds with the ability to enhance membrane material hydro-stability’s fabrication.
Co-Authors Adhe Paramita Adi Darmawan Afrisa Noor Hidayanti Agus Mirwan Ahmad Rizali Noor Akhbar Akhbar Akhbar Amalia Enggar Pratiwi Amalia Enggar Pratiwi Anna Sumardi Anna Sumardi Anna Sumardi Anna Sumardi Aptar Eka Lestari Aptar Eka Lestari Aptar Eka Lestari Aptar Eka Lestari Arfa Agustina Rezekiah Assyaifi, Zaini L Aulia Rahma Aulia Rahma Aulia Rahma Aulia Rahma Awali S. K. Harivram Awali Sir Kautsar Harivram Chairul Irawan Chairul Irawan Dewi Puspita Sari Dewi Puspita Sari Dewi Rahmawati Suparsih Dhimas Ari Pratomo Dhiyaur Rahmah Dina Amryna Chairul Putri Dina Naemah Dwi Rasy Mujiyanti Dwi Rasy Mujiyanti Elsa Nadia Pratiwi Era N R Oktaviana Erdina L. A. Rampun Erdina L.A Rampun Erdina Lulu Atika Rampun Erdina Lulu Atika Rampun Erdina Lulu Atika Rampun Erdina Lulu Atika Rampun Fitri Ria Mustalifah Fitri Ria Mustalifah Gazali, Akhmad Hesti Kesumadewi Hesti Wijayanti Isna Syauqiah Isna Syauqiah Isna Syauqiah Isna Syauqiah Isna Syauqiah Lastuti Abubakar Lilis Septyaningrum Lilis Suryani Lilis Suryani Linda Suci Wati Linda Suci Wati Linda Suciwati M. Ihsan M. Mahmud M. Topan Darmawan Mahmud Mahmud Mahmud Mahmud Mahmud Mahmud Marhamah Marhamah Maulana Wahyu Noor Ramadhan Meilana Dharma Putra Mijani Rahman, Mijani Mita Riani Rezki Mohd H. D. Othman Mufidah Nur Amalia Muhammad Hasan Albana Muhammad Roil Bilad Mustalifah, Fitri Ria Namira Ghina Safitri Nia Kania Noor, Ahmad Rizali Noor, M. Hafidhuddin Nor Aldina Norlian Ledyana Sari Nur baity Nur Riskawati Nur, Thoyib Nurhalisah Nurhalisah Nurul Huda Nurul Huda Pratiwi, Amalia E. Pratiwi, Elsa Nadia Rahma, Aulia Rahmawati Rahmawati Rampun, Erdina L.A. Rampun, Erdina Lulu Atika Rezki, Mita Riani Rian Nugraha Putra Riani Ayu Lestari Rosidah Muis Radam Sadidan Rabiah Satria Anugerah Suhendra Sazila K. Rahman SITI FATIMAH Suhendra, Satria Anugerah sunardi sunardi Syarifah Annahdliyah Thoyib Nur Tri Handayani Wahyuddin Wahyuddin Wahyuddin Wahyuddin Yanti Mawaddah Yanti Mawaddah Yanti Mawaddah Yuniarti Yuniarti Yusuf Aziz Zaini Lambri Assyaifi Zaini Lambri Assyaifi Zaini Lambri Assyaifi