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All Journal Jurnal Presipitasi : Media Komunikasi dan Pengembangan Teknik Lingkungan Jurnal Ilmu Dasar ELKHA : Jurnal Teknik Elektro Jurnal Teknik Sipil Bulletin of Chemical Reaction Engineering & Catalysis REKAYASA JC-T (Journal Cis-Trans): Jurnal Kimia dan Terapannya Indonesian Journal of Chemistry Jurnal Penelitian dan Pengabdian Kepada Masyarakat UNSIQ Unistek: Jurnal Pendidikan dan Aplikasi Industri Jurnal Teknologi Lingkungan Lahan Basah Bulletin of Chemical Reaction Engineering & Catalysis
Syahrul Khairi
Jurusan Teknik Kimia Universitas Tanjungpura
Agriculture, Biological Sciences & Forestry Automotive Engineering Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Civil Engineering, Building, Construction & Architecture Computer Science & IT Control & Systems Engineering Earth & Planetary Sciences Electrical & Electronics Engineering Energy Engineering Environmental Science Immunology & microbiology Industrial & Manufacturing Engineering Materials Science & Nanotechnology Mathematics Physics Public Health Other

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Journal : Bulletin of Chemical Reaction Engineering

 1 
Selective Hydrogenation of Biomass-derived Furfural over Supported Ni3Sn2 Alloy: Role of Supports Rodiansono Rodiansono; Maria Dewi Astuti; Syahrul Khairi; Shogo Shimazu
Bulletin of Chemical Reaction Engineering & Catalysis 2016: BCREC Volume 11 Issue 1 Year 2016 (April 2016)
Publisher : Department of Chemical Engineering - Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (739.187 KB) | DOI: 10.9767/bcrec.11.1.393.1-9

Abstract

A highly active and selective hydrogenation of biomass-derived furfural into furfuryl alcohol was achieved using supported single phase Ni3Sn2 alloy catalysts. Various supports such as active carbon (AC), g-Al2O3, Al(OH)3, ZnO, TiO2, ZrO2, MgO, Li-TN, and SiO2 have been employed in order to understand the role of the support on the formation of Ni3Sn2 alloy phase and its catalytic performance. Supported Ni3Sn2 alloy catalysts were synthesised via a simple hydrothermal treatment of the mixture of aqueous solution of nickel chloride hexahydrate and ethanol solution of tin(II) chloride dihydrate in presence of ethylene glycol at 423 K for 24 h followed by H2 treatment at 673 K for 1.5 h, then characterised by using ICP-AES, XRD, H2- and N2-adsorption. XRD profiles of samples showed that the Ni3Sn2 alloy phases are readily formed during hydrothermal processes and become clearly observed at 2θ = 43-44o after H2 treatment. The presence of Ni3Sn2 alloy species that dispersed on the supports is believed to play a key role in highly active and selective hydrogenation of biomass-derived furfural towards furfuryl alcohol. Ni3Sn2 on TiO2 and ZnO supports exhibited much lower reaction temperature to achieved >99% yield of furfuryl alcohol product compared with other supports. The effects of loading amount of Ni-Sn, reaction conditions (temperature and time profile) on the activity and selectivity towards the desired product are systematically discussed. 
Co-Authors Aini Sulastri Andreas Napitupulu Bambang Piluharto Desmaiani, Herda Eddy Kurniawan Edo Septiansyah Eric Setiawan Erlindawati Erlindawati Fitria, Laili Gayu Ika Putri Hanggara Sudrajat Herman Siagian Herudi Kandau Intan Syahbanu Iqmal Tahir Johan Sibarani Karna Wijaya Khairul Abshar Marcelina Marcelina Marcelina Marcelina, Marcelina Maria Dewi Astuti Mochammmad Meddy Danial Muhammad Rivai P Yolanda, Kristina Desideria Pradika Wibowo Raden Bayu Trisno Wijoyo Raymond Nadeak Ria Devitasari Rinjani Ratih Rakasiwi Rizki Purnaini Rodiansono Rodiansono S. Sudarko Shogo Shimazu Sri Rezeki Sri Rezeki Syafrianto, M Khalid Toto Hermanto Triandi Kuseno Trisno Wijoyo, Raden Bayu Usman A. Gani Wibowo, Pradika Wivina Diah Ivontianti Wivina Diah Ivontianti Yoeswono Yoeswono Yusup Yusup Zaky Al-Fatony